Organic Structures from 2D NMR Spectra.
Field, L. D.
Organic Structures from 2D NMR Spectra. - 1st ed. - 1 online resource (330 pages) - New York Academy of Sciences Series . - New York Academy of Sciences Series .
Cover -- Title Page -- Copyright Page -- Contents -- Preface -- List of Figures -- List of Tables -- 1 NMR Spectroscopy Basics -- 1.1 The Physics of Nuclear Spins -- 1.2 Basic NMR Instrumentation and the NMR Experiment -- 2 One-Dimensional Pulsed Fourier Transform NMR Spectroscopy -- 2.1 The Chemical Shift -- 2.2 1H NMR Spectroscopy -- 2.2.1 Chemical Shifts in 1H NMR Spectroscopy -- 2.2.2 Spin-Spin Coupling in 1H NMR Spectroscopy -- 2.2.3 Decoupling in 1H NMR Spectroscopy -- 2.2.4 The Nuclear Overhauser Effect in 1H NMR Spectroscopy -- 2.3 Carbon-13 NMR Spectroscopy -- 2.3.1 Decoupling in 13C NMR Spectroscopy -- 2.3.2 Chemical Shifts in 13C NMR Spectroscopy -- 2.4 Fluorine-19 NMR Spectroscopy -- 2.5 Phosphorus-31 NMR Spectroscopy -- 2.6 Nitrogen-15 NMR Spectroscopy -- 3 Two-Dimensional NMR Spectroscopy -- 3.1 General Principles -- 3.2 Proton-Proton Interactions -- 3.2.1 Correlation Spectroscopy - The COSY Experiment -- 3.2.2 Total Correlation Spectroscopy - The TOCSY Experiment -- 3.2.3 Nuclear Overhauser Spectroscopy - The NOESY Experiment -- 3.3 Carbon-Carbon Interactions -- 3.3.1 The INADEQUATE Experiment -- 3.4 Heteronuclear Correlation Spectroscopy -- 3.4.1 Heteronuclear Single Bond Correlation - The HSQC, HMQC and me-HSQC Experiments -- 3.4.2 Heteronuclear Multiple Bond Correlation - HMBC -- 4 Miscellaneous Topics -- 4.1 NMR Solvents -- 4.2 Reference Compounds and Standards -- 4.3 Dynamic Processes -- 4.3.1 Protons on Heteroatoms -- 4.3.2 Rotation about Partial Double Bonds -- 4.4 Second-Order Effects -- 4.5 Effect of a Chiral Centre on NMR Spectra -- 5 Worked Examples -- 5.1 General Principles -- 5.2 Worked Example 1 -- 5.3 Worked Example 2 -- 6 Problems -- Problem 1 -- Problem 2 -- Problem 3 -- Problem 4 -- Problem 5 -- Problem 6 -- Problem 7 -- Problem 8 -- Problem 9 -- Problem 10 -- Problem 11 -- Problem 12 -- Problem 13 -- Problem 14. Problem 15 -- Problem 16 -- Problem 17 -- Problem 18 -- Problem 19 -- Problem 20 -- Problem 21 -- Problem 22 -- Problem 23 -- Problem 24 -- Problem 25 -- Problem 26 -- Problem 27 -- Problem 28 -- Problem 29 -- Problem 30 -- Problem 31 -- Problem 32 -- Problem 33 -- Problem 34 -- Problem 35 -- Problem 36 -- Problem 37 -- Problem 38 -- Problem 39 -- Problem 40 -- Problem 41 -- Problem 42 -- Problem 43 -- Problem 44 -- Problem 45 -- Problem 46 -- Problem 47 -- Problem 48 -- Problem 49 -- Problem 50 -- Problem 51 -- Problem 52 -- Problem 53 -- Problem 54 -- Problem 55 -- Problem 56 -- Problem 57 -- Problem 58 -- Problem 59 -- Problem 60 -- Problem 61 -- Problem 62 -- Problem 63 -- Problem 64 -- Problem 65 -- Problem 66 -- Index -- EULA.
9781118868928
Nuclear magnetic resonance spectroscopy.
Spectrum analysis.
Electronic books.
QD96.N8 .F54 2015
543/.66
Organic Structures from 2D NMR Spectra. - 1st ed. - 1 online resource (330 pages) - New York Academy of Sciences Series . - New York Academy of Sciences Series .
Cover -- Title Page -- Copyright Page -- Contents -- Preface -- List of Figures -- List of Tables -- 1 NMR Spectroscopy Basics -- 1.1 The Physics of Nuclear Spins -- 1.2 Basic NMR Instrumentation and the NMR Experiment -- 2 One-Dimensional Pulsed Fourier Transform NMR Spectroscopy -- 2.1 The Chemical Shift -- 2.2 1H NMR Spectroscopy -- 2.2.1 Chemical Shifts in 1H NMR Spectroscopy -- 2.2.2 Spin-Spin Coupling in 1H NMR Spectroscopy -- 2.2.3 Decoupling in 1H NMR Spectroscopy -- 2.2.4 The Nuclear Overhauser Effect in 1H NMR Spectroscopy -- 2.3 Carbon-13 NMR Spectroscopy -- 2.3.1 Decoupling in 13C NMR Spectroscopy -- 2.3.2 Chemical Shifts in 13C NMR Spectroscopy -- 2.4 Fluorine-19 NMR Spectroscopy -- 2.5 Phosphorus-31 NMR Spectroscopy -- 2.6 Nitrogen-15 NMR Spectroscopy -- 3 Two-Dimensional NMR Spectroscopy -- 3.1 General Principles -- 3.2 Proton-Proton Interactions -- 3.2.1 Correlation Spectroscopy - The COSY Experiment -- 3.2.2 Total Correlation Spectroscopy - The TOCSY Experiment -- 3.2.3 Nuclear Overhauser Spectroscopy - The NOESY Experiment -- 3.3 Carbon-Carbon Interactions -- 3.3.1 The INADEQUATE Experiment -- 3.4 Heteronuclear Correlation Spectroscopy -- 3.4.1 Heteronuclear Single Bond Correlation - The HSQC, HMQC and me-HSQC Experiments -- 3.4.2 Heteronuclear Multiple Bond Correlation - HMBC -- 4 Miscellaneous Topics -- 4.1 NMR Solvents -- 4.2 Reference Compounds and Standards -- 4.3 Dynamic Processes -- 4.3.1 Protons on Heteroatoms -- 4.3.2 Rotation about Partial Double Bonds -- 4.4 Second-Order Effects -- 4.5 Effect of a Chiral Centre on NMR Spectra -- 5 Worked Examples -- 5.1 General Principles -- 5.2 Worked Example 1 -- 5.3 Worked Example 2 -- 6 Problems -- Problem 1 -- Problem 2 -- Problem 3 -- Problem 4 -- Problem 5 -- Problem 6 -- Problem 7 -- Problem 8 -- Problem 9 -- Problem 10 -- Problem 11 -- Problem 12 -- Problem 13 -- Problem 14. Problem 15 -- Problem 16 -- Problem 17 -- Problem 18 -- Problem 19 -- Problem 20 -- Problem 21 -- Problem 22 -- Problem 23 -- Problem 24 -- Problem 25 -- Problem 26 -- Problem 27 -- Problem 28 -- Problem 29 -- Problem 30 -- Problem 31 -- Problem 32 -- Problem 33 -- Problem 34 -- Problem 35 -- Problem 36 -- Problem 37 -- Problem 38 -- Problem 39 -- Problem 40 -- Problem 41 -- Problem 42 -- Problem 43 -- Problem 44 -- Problem 45 -- Problem 46 -- Problem 47 -- Problem 48 -- Problem 49 -- Problem 50 -- Problem 51 -- Problem 52 -- Problem 53 -- Problem 54 -- Problem 55 -- Problem 56 -- Problem 57 -- Problem 58 -- Problem 59 -- Problem 60 -- Problem 61 -- Problem 62 -- Problem 63 -- Problem 64 -- Problem 65 -- Problem 66 -- Index -- EULA.
9781118868928
Nuclear magnetic resonance spectroscopy.
Spectrum analysis.
Electronic books.
QD96.N8 .F54 2015
543/.66